Hydrochloric Acid → HCID 67000300, compound

Participants

Reaction Steps

The above carboxylic acid (31 mg) was dissolved in 5 mL of 4N HCl in dioxane. Within 2 min a white precipitate had formed. The mixture was stirred for 45 min and then diluted with 10 mL of methylene chloride. The solid was filtered with a filter-tipped cannula and washed with 2×10 mL of methylene chloride. The solid was dried under vacuum to provide the title compound; MS, electrospray, 339 (M+H)

Provenance & Evidence