Hydrochloric Acid → HCID 66999370, compound

Participants

Reaction Steps

The above carboxylic acid (31 mg) was dissolved in 10 mL of 4N HCl in dioxane. The mixture was spun on the rotovap without vacuum for 45 min. The solid was filtered with a filter-tipped cannula and washed with 2×10 mL of methylene chloride. The solid was dried under vacuum to yield the title compound (21 mg); MS, electrospray, 278 (M+H).

Provenance & Evidence