Cyclobutanone → HCID 59197929, compound

HRID 560208Notes

Reaction equation

[N:1]1([C:6]2([C:10]#[N:11])[CH2:9]O[CH2:7]2)[CH2:5][CH2:4][CH2:3][CH2:2]1.[C:12]1(=O)CCC1.[CH3:17][N:18]1CCNCC1>>[CH3:17][N:18]1[CH2:4][CH2:5][N:1]([C:6]2([C:10]#[N:11])[CH2:9][CH2:12][CH2:7]2)[CH2:2][CH2:3]1

Participants

Reactant 3

HCID 14496Cyclobutanone

HCID 531671-Methylpiperazine

HCID 591979193-Cyano-3-(pyrrolidin-1-YL)oxetane

Product 1

HCID 59197929HCID 59197929, compound

Procedure

The title compound, light yellow liquid, MS: m/e=180.2 [(M+H)+], was prepared in accordance with the general method of intermediate A from cyclobutanone and 1-methylpiperazine.

Sources & evidence

ORD record: ord-943bd93e73a94c669a731130935670df
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063098B2

Reaction notes

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