HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 13060114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 57489315 | HCID 57489315 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 13060114 | HCID 13060114 | — |
Reaction Steps
A mixture of 2-(2,2-diethoxy-ethylsulfanyl)-5-methyl-1H-imidazole-4-carboxylic acid ethyl ester (10.0 mmol) in aq. HCl (15%, 8.0 mL) is stirred for 1 h at RT and neutralized by addition of aq. Na2CO3 solution. The obtained precipitate is filtered off to give the desired product which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063099B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-309e4bc79f0d4915bf7b87c578900f3b |
| Source note | uspto-grants-2011_11 |