HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59717983, compound → HCID 59717968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59717983 | HCID 59717983 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 59717968 | HCID 59717968 | 120.1% |
Reaction Steps
4-[5-(2-Methyl-cyclohexylcarbamoyl)-naphthalene-1-sulfonylamino]-piperidine-1-carboxylic acid tert-butyl ester 47 (380 mg) was dissolved in 4N HCl/dioxane (10 mL) and stirred for 3 hours at room temperature. Concentration in vacuo afforded 48 (370 mg) as its hydrochloride salt that was used without further purification. LC/MS m/z 430 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063222B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-cedbc0335b53410e80872060e39ae8e6 |
| Source note | uspto-grants-2011_11 |