HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 45117210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 66999255 | HCID 66999255 | — |
| Product | HCID 45117210 | HCID 45117210 | — |
Reaction Steps
1N NaOH (5 ml) was added to a solution of the ester in dioxan (5 ml) and the solution is stirred at r.t. overnight. After evaporation of the organic solvent, the mixture is acidified to pH=2 with 2N HCl until complete precipitation of the product, which is isolated, as a white solid by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063242B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6c71b272e5f64896841a24016ed5d907 |
| Source note | uspto-grants-2011_11 |