HRID561581

反应详情

EQUATION

反应方程式

HRID 561581 的结构方程式

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

The title compound was prepared starting from 500 mg (2.56 mmol) of the compound from Example 8 and 605 mg (2.82 mmol) of the compound from Example 79A in analogy to the synthesis of the compound from Example 95. As a difference, the reaction mixture was stirred at 0° C. for 2 h and then warmed to RT. 67 mg (7% of theory) of the target compound were obtained.

WORKUP

后处理

  1. temperaturewarmed to RT
  2. custom67 mg (7% of theory) of the target compound were obtained