HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2,2,4,4,6,6-Hexamethylcyclotrisilazane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Dichlorodimethylsilane | HCID 6398 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2,2,4,4,6,6-Hexamethylcyclotrisilazane | HCID 66094 | — |
Reaction Steps
This method involves reacting dimethyldichlorosilane with ammonia in benzene at 30° C., removing ammonia chloride by-product by filtration through a glass filter or the like, and distilling the reaction product to isolate hexamethylcyclotrisilazane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05245066 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-c1c083a6f395481abe3df8731345c900 |
| Source note | uspto-grants-1993_09 |