HRID561708

反应详情

EQUATION

反应方程式

HRID 561708 的结构方程式

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

The title compound was prepared starting from 500 mg (2.56 mmol) of the compound from Example 11A and 667 mg (2.56 mmol) of the compound from Example 81A in analogy to the synthesis of the compound from Example 278. A difference was that stirring at 80° C. was for only 4 h. 535 mg (50% of theory) of the target compound were obtained.

WORKUP

后处理

  1. custom535 mg (50% of theory) of the target compound were obtained