HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22467254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | Ethyl 4-chloro-3-methylphenol | HCID 22134509 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22467254 | HCID 22467254 | — |
Reaction Steps
To a solution of ethyl 4-chloro-3-methylphenol (1 eq.) in acetone (0.2 M) was added potassium carbonate (5 eq.) and 1-bromo-2-methoxyethane (1.3 eq.). The resulting suspension was refluxed for 25 h. The insolubles were removed via filtration and the filtrate was concentrated in vacuo to furnish the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063105B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-224af951c7104183870510e77339fa69 |
| Source note | uspto-grants-2011_11 |