HRID561793

反应详情

EQUATION

反应方程式

HRID 561793 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of ethyl 4-chloro-3-methylphenol (1 eq.) in acetone (0.2 M) was added potassium carbonate (5 eq.) and 1-bromo-2-methoxyethane (1.3 eq.). The resulting suspension was refluxed for 25 h. The insolubles were removed via filtration and the filtrate was concentrated in vacuo to furnish the title compound.

WORKUP

后处理

  1. temperatureThe resulting suspension was refluxed for 25 h
  2. customThe insolubles were removed via filtration
  3. concentrationthe filtrate was concentrated in vacuo