HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-4-(methylamino)piperidine → HCID 67000733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-4-(methylamino)piperidine | HCID 566323 | — |
| Reactant | HCID 66722800 | HCID 66722800 | — |
| Product | HCID 67000733 | HCID 67000733 | 42.5% |
Reaction Steps
The title compound was prepared according to the general procedure for 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(5-{[methyl(1-methyl-4-piperidinyl)amino]methyl}-3-thienyl)-1H-indole-7-carboxamide trifluoroacetate, substituting 3-(methylamino)propanenitrile (84.12 mg, 1.0 mmol) for N,1-dimethyl-4-piperidinamine to afford 24 mg of the title compound (42.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-808208bde3b349b5811785b3ab58bd2a |
| Source note | uspto-grants-2011_11 |