HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 90030960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 90031188 | HCID 90031188 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90030960 | HCID 90030960 | — |
Reaction Steps
A mixture of N-(1-((3-cyanophenoxy)methyl)-1H-indol-6-yl)-3-oxobutanamide (1.04 g, 2.99 mmol), MeOH (20 mL) and ammonia (20 mL) was stirred at rt overnight. The mixture was concentrated in vacuo to give the title compound, which was used for next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434695B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-e727c143835b4fac9db5b24131a6215e |
| Source note | uspto-grants-2016_09 |