HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 562407Generated: October 31, 2026
Bromotrimethylsilane → HCID 66832668, compound
https://huagongshe.com/reaction/562407
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 86618280 | HCID 86618280 | — |
| Product | HCID 66832668 | HCID 66832668 | — |
Reaction Steps
Bromotrimethylsilane (43 mL, 0.326 mol) was added dropwise to cyclopropylmethyl-phosphonic acid diisopropyl ester (18.00 g, 81.8 mmol) stirred in a reaction flask chilled to 5° C. The resulting solution was allowed to warm to ambient temperature, stirred for three hours, and then concentrated by rotary evaporation yielding crude cyclopropylmethyl-phosphonic acid bis(trimethylsilyl) ester which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08067395B2 |
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| Source dataset | uspto-grants-2011_11 |
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| ORD ID | ord-2ccaeb84dec146f2ab077bd6e903d1dd |
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| Source note | uspto-grants-2011_11 |
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