化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 3-Bromo-4-hydroxyphenylacetic acid | HCID 2769628 | — |
| 生成物 | Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate | HCID 18620106 | — |
反応手順
(3-Bromo-4-hydroxy-phenyl)-acetic acid (5.6 mmol) in EtOH (20 mL) was treated with sulfuric acid (1 mL) and stirred at room temperature over the weekend. The mixture was concentrated to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08067445B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-434516121a0b4996ae885f5f0b5347c6 |
| 出典メモ | uspto-grants-2011_11 |