HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → 3,5-Dichlorobenzyl Chloroformate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 3,5-Dichlorobenzylic alcohol | HCID 43236 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3,5-Dichlorobenzyl Chloroformate | HCID 13305532 | — |
Reaction Steps
To 3,5-dichlorobenzyl alcohol (0.201 g, 1.06 mmol) in CH2Cl2 (0.5 mL) was added phosgene (20% in toluene; 0.42 mL, 0.79 mmol), and the mixture was stirred at room temperature for 30 minutes to give the title compound, which was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08067445B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-653d9b24318b4ce58c5b4d26d8b885b1 |
| Source note | uspto-grants-2011_11 |