Phosgene → (4-Chlorophenyl)methyl chloroformate

HRID 563587Notes

Reaction equation

HRID 563587 reaction equation
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][OH:7])=[CH:4][CH:3]=1.[C:10](Cl)([Cl:12])=[O:11]>>[Cl:12][C:10]([O:7][CH2:6][C:5]1[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=1)=[O:11]

Participants

3

Reactant 2

HCID 6371PhosgeneHCID 133974-Chlorobenzyl alcohol

Product 1

HCID 13292914(4-Chlorophenyl)methyl chloroformate

Procedure

Prepared according to the procedure described in Example 56, Step 1, using the following starting materials: 4-chlorobenzyl alcohol and phosgene (20% in toluene).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f429bb9f906a42fc8086fd38126e7155
Source dataset
uspto-grants-2011_11
Patent number
US08067445B2

Reaction notes

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