2-Bromoethyl ethyl ether → HCID 66744353, compound

Participants

Reaction Steps

The synthesis of FEA was carried out in a manner similar to that of BnEO (process 2) using N-ethylbenzylamine (15 mL, 0.101 mol), bromoethyl ethyl ether (17 mL, 0.101×1.5 mol), and ethanol (100 mL) as a solvent. BnEE (12.79 g, 61.69 mmol, yield 61%) was obtained as a pale yellow clear liquid. [Purification was carried out by medium pressure silica gel column chromatography (ethyl acetate:n-hexane=4:1).]

Provenance & Evidence