反应详情

A mixture of 91 mg (0.24 mmol) 6-methoxy-1-[2-(4-trifluoromethyl-phenyl)-ethyl]-4,9-dihydro-3H-β-carboline and 27.7 mg (0.73 mmol) sodium borohydride in 5 mL ethanol was stirred for 2 h at room temperature. The mixture was filtered and evaporated to dryness. Trituration with ethyl acetate yielded after drying 90 mg (98%) of the title compound as light yellow solid.

1. filtrationThe mixture was filtered
2. customevaporated to dryness
3. customTrituration with ethyl acetate yielded
4. dry with materialafter drying 90 mg (98%) of the title compound as light yellow solid