HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-Amino-3,5-dinitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Chloro-3,5-dinitropyridine | HCID 75738 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-3,5-dinitropyridine | HCID 504340 | — |
Reaction Steps
To a solution of 25 g 2-Chloro-3,5-dinitropyridine in 190 ml ethanol were added dropwise 75 ml concentrated ammonia at room temperature. After stirring for 1 hour (hr), the mixture was cooled in an ice bath. The product was isolated by filtration and washed with cold water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08067599B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-f591333097c54192914a348203b76141 |
| Source note | uspto-grants-2011_11 |