HCID 178426700, compound → HCID 178426380, compound

Participants

Reaction Steps

0.75 g of N-(3H-Imidazo[4,5-b]pyridin-6-yl)-2-methyl-5-nitro-benzamide in 20 ml methanol were hydrogenated over 10% palladium on charcoal at room temperature and atmospheric pressure. After 3 hrs conversion was complete as judged by HPLC/MS and the catalyst was filtered off. The filtrate was evaporated and the residue was used without further purification for the next steps.

Provenance & Evidence