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HRID564056

反应详情

EQUATION

反应方程式

HRID 564056 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)Cl)cc1
HCID7397

p-Toluenesulfonyl chloride

C7H7ClO2S

结构：CC(C)(C)OC(=O)N1CCc2cc(CCO)ccc2C1
HCID67006783

1,1-Dimethylethyl 3,4-dihydro-6-(2-hydroxyethyl)-2(1H)-isoquinolinecarboxylate

C16H23NO3

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)OCCc2ccc3c(c2)CCN(C(=O)OC(C)(C)C)C3)cc1
HCID58042794

未命名化合物

PROCEDURE

实验过程

6-[2-(Toluene-4-sulfonyloxy)-ethyl]-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester is prepared as example 7d from 1.60 g (5.77 mmol) 6-(2-hydroxy-ethyl)-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester (preparation 10b) and 1.21 g (6.35 mmol) 4-methyl-benzenesulfonyl chloride.