HRID564762

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1nccn1C

HCID2763252

1-Methyl-2-(tributylstannyl)-1H-imidazole

C16H32N2Sn

结构：Clc1cc2c(Nc3ccc(OCc4ccccc4)cc3)ncnc2cn1

HCID21952168

未命名化合物

PRODUCTS

生成物

结构：Cn1ccnc1-c1cc2c(Nc3ccc(OCc4ccccc4)cc3)ncnc2cn1

HCID22112889

未命名化合物

PROCEDURE

实验过程

Prepared according to Procedure B from 4-(4-benzyloxyanilino)-6-chloropyrido[3,4-d]pyrimidine and 2-(tri-n-butylstannyl)-N-methylimidazole (prepared according to the published method: J. Organometallic Chem., (1989), 61); δH [2H6]-DMSO 10.35 (1H,s), 9.17 (1H,s), 9.13 (1H,s), 8.65 (1H, s), 7.79 (2H,d), 7.32-7.55 (6H,m), 7.13 (1H,s), 7.09 (2H,d), 5.16 (2H,s), 4.10 (3H,s); m/z (M+1)+409.

WORKUP

后处理

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