1-Methyl-2-(tributylstannyl)-1H-imidazole → HCID 22112889, compound

Participants

Role	Name	HCID	Charge
Reactant	1-Methyl-2-(tributylstannyl)-1H-imidazole	HCID 2763252	—
Reactant	4-(4-Benzyloxyanilino)6-chloropyrido[3,4-d]pyrimidine	HCID 21952168	—
Product	HCID 22112889	HCID 22112889	—

Reaction Steps

Prepared according to Procedure B from 4-(4-benzyloxyanilino)-6-chloropyrido[3,4-d]pyrimidine and 2-(tri-n-butylstannyl)-N-methylimidazole (prepared according to the published method: J. Organometallic Chem., (1989), 61); δH [2H6]-DMSO 10.35 (1H,s), 9.17 (1H,s), 9.13 (1H,s), 8.65 (1H, s), 7.79 (2H,d), 7.32-7.55 (6H,m), 7.13 (1H,s), 7.09 (2H,d), 5.16 (2H,s), 4.10 (3H,s); m/z (M+1)+409.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06169091A
Source dataset	uspto-grants-2001_01
ORD ID	ord-b6e1153ffc0d4d9c9ecae39b190bdb68
Source note	uspto-grants-2001_01