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HRID564794

反应详情

EQUATION

反应方程式

HRID 564794 的结构方程式

REACTANTS

反应物

4
结构：N
HCID222

Ammonia gas

H3N

结构：ClCCl
HCID6344

Dichloromethane

CH2Cl2

结构：Nc1ccc(OCc2ccccc2)c(Cl)c1
HCID1268285

4-Benzyloxy-3-chloroaniline

C13H12ClNO

结构：CN(C)c1cc2c(Cl)ncnc2cn1
HCID22727453

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1cc2c(Nc3ccc(OCc4ccccc4)c(Cl)c3)ncnc2cn1.Cl
HCID22112884

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Prepared according to Procedure A from 4-chloro-6-(N,N-dimethylamino)pyrido[3,4-d]pyrimidine and 4-benzyloxy-3-chloroaniline (prepared according to the published method: WO96/09294); tlc (dichloromethane:ethanol:aq. ammonia, 100:8:1) Rf 0.48; m/z (M+1)+406.

WORKUP

后处理

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