HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21267689, compound → HCID 21267691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21267689 | HCID 21267689 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21267691 | HCID 21267691 | 102% |
Reaction Steps
3.05 g (12.0 mmol) 4-nitro-2,5-diethoxyphenethylamine N6 was dissolved in 50 ml ethanol, and 1.5 g 10% palladium on carbon black was added. This suspension was hydrogenated at 2.2 atm. for 18 hours, till no more hydrogen uptake was observed. The catalyst was filtered off and the solvent was evaporated to afford 2.75 g light yellow oil (yield: 102%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06171866B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-47eca309facf4511b991ad4c8833121e |
| Source note | uspto-grants-2001_01 |