HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester → HCID 18416776, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester | HCID 54357246 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Sodium Hydroxide | HCID 14798 | — |
| Produkt | HCID 18416776 | HCID 18416776 | — |
Reaktionsschritte
2-(4-Methoxy-phenylsulfanyl)-heptanoic acid was prepared starting with 2-(4-methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (4 g, 13.5 mmol) dissolved in methanol (300 ml) and 10 N NaOH (25 ml). The resulting reaction mixture was worked up as outlined in example 1. Yield 3 g (83%). yellow oil. MS: 267.1 (M−H)−.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06172057B2 |
| Quelldatensatz | uspto-grants-2001_01 |
| ORD ID | ord-7503fe6965844efca9b83df27e74af25 |
| Quellennotiz | uspto-grants-2001_01 |