HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 21268360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | HCID 15411835 | HCID 15411835 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21268360 | HCID 21268360 | — |
Reaction Steps
Oxidation of 8-(decahydro-azulen-2-yl)-1-phenyl-1,8-diaza-spiro[4.5]decan-4-ol (mixture of diastereoisomers) according to the general method of example 20 and formation of the fumarate with fumaric acid in diethyl ether yielded the title compound, pale brown solid, m.p. 219° C. and MS: m/e=367.3 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172075B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-c118da31ddc747bc9674c100eb310e89 |
| Source note | uspto-grants-2001_01 |