HRID565395

反应详情

EQUATION

反应方程式

HRID 565395 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

cis-1-(4-Isopropyl-cyclohexyl)-piperidine-4-one (5.0 g, 23.4 mmol), aniline (3.3 g, 35.3 mmol) and molecular sieves (20 g, 4A) were stirred in 100 ml pentane at room temperature for 6 days. The molecular sieves were filtered off and the solvent was evaporated. The crude product was used without any further purification.

WORKUP

后处理

  1. filtrationThe molecular sieves were filtered off
  2. customthe solvent was evaporated
  3. customThe crude product was used without any further purification