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HRID56558

反应详情

EQUATION

反应方程式

HRID 56558 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(-c2ccco2)cc(OC)c1Br
HCID58431988

未命名化合物

结构：COC(C(=O)N(C)OC)c1ccc(-c2nnc(C)s2)cc1
HCID58431997

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(-c2ccc(C(=O)C(OC)c3ccc(-c4nnc(C)s4)cc3)o2)cc(OC)c1Br
HCID53363484

未命名化合物

PROCEDURE

实验过程

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-methoxy-2-(4-(5-methyl-1,3,4-thiadiazol-2-yl)phenyl)ethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and N,2-dimethoxy-N-methyl-2-(4-(5-methyl-1,3,4-thiadiazol-2-yl)phenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (70% EtOAc/hexanes) gave the product as a pale yellow solid (0.044 g, 15% yield). MS: m/z 529.3 [M+H]+.

WORKUP

后处理

  1. customPurification by chromatography (70% EtOAc/hexanes)