Piperazine → HCID 22111113, compound

HRID 565638Notes

Reaction equation

HRID 565638 reaction equation
[C:1]1([CH:7]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1>>[C:1]1([CH:7]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][N:22]2[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 4837PiperazineHCID 17895888HCID 17895888, compound

Product 1

HCID 22111113HCID 22111113, compoundYield 94%

Procedure

Using 6-(dipenylmethoxy)hexyl chloride and piperazine, the procedure of Reference Example 16 was otherwise repeated to provide the title compound.

Sources & evidence

ORD record
ord-a847bb527455410aad24aac01be6c378
Source dataset
uspto-grants-2001_01
Patent number
US06172085B2

Reaction notes

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