HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Bromo-3,5-dimethoxyphenyl)furan → 1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Bromo-3,5-dimethoxyphenyl)furan | HCID 58431988 | — |
| Reactant | 2-(4-((dimethylamino)methyl)phenyl)-N,2-dimethoxy-N-methylacetamide | HCID 58432061 | — |
| Product | 1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone | HCID 58432105 | — |
Reaction Steps
1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-(4-((dimethylamino)methyl)phenyl)-N,2-dimethoxy-N-methylacetamide according to the procedure used in Example 30. Purification by chromatography (4% MeOH/CH2Cl2) gave the product as a pale yellow oil (0.004 g, 1% yield). MS: ink 488.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434707B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-35e3bd28dd4746e19e09cf522da5ed4b |
| Source note | uspto-grants-2016_09 |