HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N-(3-Chlorophenyl)benzenemethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 86756217 | HCID 86756217 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N-(3-Chlorophenyl)benzenemethanamine | HCID 11506782 | 96.7% |
Reaction Steps
Next, (+)-(3-chlorophenyl)phenylmethylamine (+)tartrate (4.28 g) was suspended in chloroform (40 ml), and 28%-aqueous ammonia was added thereto to neutralize the mixture. Thereafter, the chloroform layer was separated therefrom. The extract was dried over anhydrous magnesium sulfate, and the solvent was removed by evaporation in vacuo, to give (+)-(3-chlorophenyl)phenylmethylamine (2.45 g) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172228B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-c26e0cf2cd824304818775200eedf1f3 |
| Source note | uspto-grants-2001_01 |