HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-bromobenzenemethanol → 2-Amino-5-bromobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-bromobenzenemethanol | HCID 11030874 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Amino-5-bromobenzaldehyde | HCID 23510475 | 71.1% |
Reaction Steps
To acetone (300 ml) were added (2-amino-5-bromophenyl)methanol (23.32 g) and active manganese dioxide (58.5 g), and the mixture was stirred at room temperature for 17.5 hours and filtered. The solvent was evaporated under reduced pressure to give 2-amino-5-bromobenzaldehyde (16.41 g, 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172061B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-65c40bbacbb4473ebb9494df3de6cedb |
| Source note | uspto-grants-2001_01 |