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HRID566318

反应详情

EQUATION

反应方程式

HRID 566318 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCC(C)=O
HCID8093

2-Octanone

C8H16O

结构：CC(C)(C)OC(=O)NN
HCID70091

Hydrazinecarboxylic acid, 1,1-dimethylethyl ester

C5H12N2O2

PRODUCTS

生成物

1
结构：CCCCCCC(C)=NNC(=O)OC(C)(C)C
HCID72599198

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCCCC1
溶剂HCID8078

Cyclohexane

C6H12

PROCEDURE

实验过程

40 g (312 mmol) of 2-octanone and 41.23 g (312 mmol) of tert-butyl carbazate are refluxed for 2 hours in 350 ml of cyclohexane. The solvent and water are removed in vacuo. This gives 74.10 g (98%) of a waxy solid.

WORKUP

后处理

  1. customThe solvent and water are removed in vacuo