HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Octanone → tert-Butyl N'-(1-methyl-heptylidene)-hydrazinecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Octanone | HCID 8093 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | tert-Butyl N'-(1-methyl-heptylidene)-hydrazinecarboxylate | HCID 72599198 | — |
Reaction Steps
40 g (312 mmol) of 2-octanone and 41.23 g (312 mmol) of tert-butyl carbazate are refluxed for 2 hours in 350 ml of cyclohexane. The solvent and water are removed in vacuo. This gives 74.10 g (98%) of a waxy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174884B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-e0b12e0f9acd4b18a123b7e768916f98 |
| Source note | uspto-grants-2001_01 |