Hydrogen chloride-ethyl acetate → HCID 88146823, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.19 ml) was added to a solution of [6-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]-3-cyclohexenyl]-N-octadecylformamide (0.20 g) in ethyl acetate (4 ml) while being cooled with ice and then stirred for 10 minutes. The deposited crystals were dissolved in ethanol and concentrated. The residue was crystallized with ethyl acetate, thereby yielding the entitled compound (0.21 g) as white crystals.

Provenance & Evidence