HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 88145729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 88145730 | HCID 88145730 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 88145729 | HCID 88145729 | — |
Reaction Steps
4N Hydrochloric acid/ethyl acetate solution (0.26 ml) was added to a solution of [6-[[N-(3-morpholinopropyl)carbamoyloxy]methyl]-3-cyclohexenyl]-N-octadecylformamide (0.30 g) in ethyl acetate (4 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was crystallized with ethyl acetate, thereby yielding the entitled compound (0.26 g) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174885B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-2cf799600c7a418eb44b985b8239b9d7 |
| Source note | uspto-grants-2001_01 |