HCID 9916894, compound → HCID 21266130, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.28 ml) was added to a solution of {6-[(octadecylamino)carbonyl]-3-cyclohexenyl}methyl 4-benzyltetrahydro-1(2H)-pyrazine carboxylate (2.600 g) in ethyl acetate (26 ml). After being stirred for half an hour at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate-ethanol mixed solution, thereby yielding the entitled compound (2.412 g) as white solid.

Provenance & Evidence