HCID 21265690, compound → HCID 17903582, compound

Participants

Reaction Steps

A solution of methyl 3-(benzylamino)-2,2-di{4-[(di-tert-butoxyphosphoryl)(difluoro)methyl]benzyl}-3-oxopropanoate (15 mg) in 2 mL of CH2Cl2 and 1.5 mL of TFA was stirred for 2 h and then concentrated. The residue was dissolved in 3 mL of water and washed with 3×2 mL of ether and the aqueous solution was lyopholized to give 13 mg of the title compound as a white solid.

Provenance & Evidence