HRID56653

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CCC(C(=O)OC(C)(C)C)n1ccc(-c2cc(Cl)ccc2C#N)cc1=O

HCID117622863

未命名化合物

PRODUCTS

生成物

结构：CCC(C(=O)O)n1ccc(-c2cc(Cl)ccc2C#N)cc1=O

HCID117622746

未命名化合物

PROCEDURE

实验过程

543 mg (purity 59%, 0.86 mmol) of tert-butyl 2-[4-(5-chloro-2-cyanophenyl)-2-oxopyridin-1(2H)-yl]butanoate (racemate) were hydrolysed with 20 eq. of TFA according to General Method 6A. Yield: 425 mg (purity 60%, 94% of theory)