HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 1,1'-(3-Bromoprop-1-ene-1,1-diyl)dibenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1,1-Diphenyl-1-propene | HCID 238207 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 1,1'-(3-Bromoprop-1-ene-1,1-diyl)dibenzene | HCID 12346545 | — |
Reaction Steps
A mixture of 1,1-diphenyl-1-propene (17.0 g, 0.10 mol), carbontetrachloride (100 ml), benzoylperoxide (0.2 g) and N-bromosuccinimide (17.8 g, 0.10 mol) was heated at reflux temperature for 18 h. The reaction mixture was allowed to cool to room temperature, filtered and the solvent was evaporated in vacuo to give 3-bromo-1, 1-diphenyl-1-propene in a quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174898B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-af3f193276504907b8aa0a030f1ba784 |
| Source note | uspto-grants-2001_01 |