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HRID56656

反应详情

EQUATION

反应方程式

HRID 56656 的结构方程式

REACTANTS

反应物

2
结构：[Li+].[OH-]
HCID3939

Lithium hydroxide anhydrous

HLiO

结构：CCOC(=O)C(C(C)C)n1ccc(-c2cc(Cl)ccc2C#N)cc1=O
HCID117622646

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)C(C(=O)O)n1ccc(-c2cc(Cl)ccc2C#N)cc1=O
HCID117622685

未命名化合物

PROCEDURE

实验过程

117 mg (purity 81%, 0.26 mmol) of ethyl 2-[4-(5-chloro-2-cyanophenyl)-2-oxopyridin-1(2H)-yl]-3-methylbutanoate (racemate) were hydrolysed with lithium hydroxide according to General Method 6B. Yield: 79 mg (purity 86%, 78% of theory)