Diphosgene → HCID 57052211, compound

HRID 566606Notes

Reaction equation

HRID 566606 reaction equation
[CH2:1]([O:3][N:4]=[CH:5][C:6]1[CH:11]=[C:10]([NH2:12])[C:9]([Cl:13])=[CH:8][C:7]=1[Cl:14])[CH3:2].[O:15]=[C:16](Cl)OC(Cl)(Cl)Cl>>[CH2:1]([O:3][N:4]=[CH:5][C:6]1[CH:11]=[C:10]([N:12]=[C:16]=[O:15])[C:9]([Cl:13])=[CH:8][C:7]=1[Cl:14])[CH3:2]

Participants

3

Reactant 2

HCID 10426DiphosgeneHCID 54281623HCID 54281623, compound

Product 1

HCID 57052211HCID 57052211, compound

Procedure

65.3 g (0.28 mol) of 5-amino-2,4-dichlorobenzaldehyde (O-ethyl)-oxime (obtainable by the process given for precursors 28.1-28.3) and 60.9 g (0.31 mol) of diphosgene were reacted in the manner described for precursor 3.1. Yield: 72.9 g.

Workup

  1. customwere reacted in the manner

Sources & evidence

ORD record
ord-a3f0b4bcf2ed4d3480d85fd84ba60bb2
Source dataset
uspto-grants-2001_01
Patent number
US06175007B1

Reaction notes

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