HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54207148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 3-amino-4,4,4-trifluorocrotonate | HCID 5702529 | — |
| Reactant | HCID 57052211 | HCID 57052211 | — |
| Product | HCID 54207148 | HCID 54207148 | — |
Reaction Steps
9.2 g (0.31 mol) of sodium hydride, 51.3 g (0.28 mol) of ethyl 3-amino-4,4,4-trifluorocrotonate and 72.6 g (0.28 mol) of 2,4-dichloro-5-isocyanatobenzaldehyde (O-ethyl)oxime were reacted in the manner described for precursor 3.2. Yield: 72.0 g; m.p.: 205-209° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06175007B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-028caa2ab41d4ae1a00625cadb1f08ff |
| Source note | uspto-grants-2001_01 |