HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 57092186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 54207148 | HCID 54207148 | — |
| Product | HCID 57092186 | HCID 57092186 | — |
Reaction Steps
69.3 g (0.175 mol) of 2,4-dichloro-5-(6-trifluoromethyl-2,4(1H,3H)-pyrimidinedion-3-yl)benzaldehyde (O-ethyl)oxime, 26.6 g (0.19 mol) of potassium carbonate and 27.3 g (0.19 mol) of methyl iodide were reacted in the manner described for precursor 3.3. Yield: 69.0 g; m.p.: 140-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06175007B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-5757ef8c6d4846acbe585ce969a1a3b0 |
| Source note | uspto-grants-2001_01 |