Ammonium Hydroxide → [4,4'-Bipyridin]-2-amine

HRID 566725노트

반응식

HRID 566725 반응식
Cl[C:2]1[CH:7]=[C:6]([C:8]2[CH:13]=[CH:12][N:11]=[CH:10][CH:9]=2)[CH:5]=[CH:4][N:3]=1.[NH4+:14].[OH-]>>[NH2:14][C:2]1[CH:7]=[C:6]([C:8]2[CH:13]=[CH:12][N:11]=[CH:10][CH:9]=2)[CH:5]=[CH:4][N:3]=1

참가 물질

3

반응물 2

HCID 14923Ammonium HydroxideHCID 135337182-Chloro-4,4'-bipyridine

생성물 1

HCID 21912841[4,4'-Bipyridin]-2-amine

실험 절차

The title compound was prepared by heating 2-chloro-[4,4′]bipyridinyl and NH4OH (30% in H2O) in a bomb at 210° C. for 48 hours: MS (m/z): Calcd. C10H9N3 (M+): 171, found (M+H)+: 172.1

출처 및 근거

ORD 기록
ord-df937a230c784ba7a9553999e5877cf9
출처 데이터셋
uspto-grants-2001_01
특허 번호
US06174901B1

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