HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → [4,4'-Bipyridin]-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Chloro-4,4'-bipyridine | HCID 13533718 | — |
| Product | [4,4'-Bipyridin]-2-amine | HCID 21912841 | — |
Reaction Steps
The title compound was prepared by heating 2-chloro-[4,4′]bipyridinyl and NH4OH (30% in H2O) in a bomb at 210° C. for 48 hours: MS (m/z): Calcd. C10H9N3 (M+): 171, found (M+H)+: 172.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174901B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-df937a230c784ba7a9553999e5877cf9 |
| Source note | uspto-grants-2001_01 |