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HRID56681

反应详情

EQUATION

反应方程式

HRID 56681 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1cc(Cl)ccc1Br
HCID44558136

(2-Bromo-5-chlorophenyl)boronic acid

C6H5BBrClO2

结构：CC(C)(C)OC(=O)Cn1ccc(Br)cc1=O
HCID117622649

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Cn1ccc(-c2cc(Cl)ccc2Br)cc1=O
HCID117622756

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccc([P](c2ccccc2)(c2ccccc2)[Pd]([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)[P](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
催化剂HCID178418397

未命名化合物

PROCEDURE

实验过程

3.8 g (12 mmol) of tert-butyl (4-bromo-2-oxopyridin-1(2H)-yl)acetate and 3.4 g (14.4 mmol) of 2-bromo-5-chlorophenylboronic acid in the presence of tetrakis(triphenylphosphine)palladium(0) were reacted according to General Method 2A. Yield: 3.9 g (purity 94%, 76% of theory)