Hydrochloric Acid → HCID 70219239, compound

Participants

Reaction Steps

To an ethyl acetate solution (25 ml) containing 2.500 g of 2,2-dimethyl-3-{[(octadecylamino)carbonyl]oxy}propyl 4-methyltetrahydro-1(2H)-pyrazinecarboxylate was added 1.42 ml of a 4N hydrogen chloride solution in ethyl acetate, followed by stirring at room temperature for 0.5 hour. After the reaction mixture was concentrated under reduced pressure, the resulting residue was recrystallized from a mixture of ethanol and ethyl acetate to obtain 2.323 g of the title compound in the form of a white solid.

Provenance & Evidence